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Shelf life study has a protocol and provides the results of shelf life studies of tobacco products over time with different conditions and analytes.  Generally there are many conditions with at least two with varying temperature, humidity, etc.

The initial table shows the a number of the analytes and test conditions used in Shelf Life studies for tobacco products for one testing condition at one timepoint and one replicate.


For Specimen - could use Plant based material; Synthetic material (codelist has swabbed material); For Specimen Condition- could use DRIED, FRESH, CONCENTRATED,

Row 1:Shows the LBTEST of Product Moisture which reflects the percentage of moisture in the substance for the condition noted in LBTSTCND which is Condition 1 (X°C/ Z% RH). Product Moisture is sometimes referred to as "Oven Volatiles".
 explain the spec condition and as-is and DWB - NNN-as is an NNN-DWB
Rows 2-12:Show the analytes used in testing.

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lb.xpt

lb.xpt

RowSTUDYIDDOMAINLBSEQLBREFIDLBSPIDLBTESTCDLBTESTLBTSTCNDLBORRESLBORRESULBSTRESCLBSTRESNLBSTRESULBSPECLBSPCCNDLBMETHODLBANMETHLBTMTHSNLBSTNRCLBREPNUMLBTPTLBTPTNUM
1TOB07LB1


Product MoistureCondition 1 (X°C/ Z% RH)
%

%TOBACCO PRODUCTFRESH



1Week 01
2TOB07LB2


pHCondition 1 (X°C/ Z% RH)




TOBACCO PRODUCTFRESH



1Week 01
3TOB07LB3


Water ActivityCondition 1 (X°C/ Z% RH)




TOBACCO PRODUCTFRESH



1Week 01
4TOB07LB4


NNK-as isCondition 1 (X°C/ Z% RH)
ng/g

ng/gTOBACCO PRODUCTFRESH



1Week 01
5TOB07LB5


NNKCondition 1 (X°C/ Z% RH)
ng/g

ng/gTOBACCO PRODUCTDRIED



1Week 01
6TOB07LB6


NNNCondition 1 (X°C/ Z% RH)
ng/g

ng/gTOBACCO PRODUCTFRESH



1Week 01
7TOB07LB7


NNN-DWBCondition 1 (X°C/ Z% RH)
ng/g

ng/gTOBACCO PRODUCTDRIED



1Week 01
8TOB07LB8


TSNA -as isCondition 1 (X°C/ Z% RH)
ng/g

ng/gTOBACCO PRODUCTFRESH



1Week 01
9TOB07LB9


TSNA -DWBCondition 1 (X°C/ Z% RH)
ng/g

ng/gTOBACCO PRODUCTDRIED



1Week 01
10TOB07LB10


Aerobic Plate CountCondition 1 (X°C/ Z% RH)




TOBACCO PRODUCTFRESH



1Week 01
11TOB07LB11


MoldCondition 1 (X°C/ Z% RH)




TOBACCO PRODUCTFRESH



1Week 01
12TOB07LB12


YeastCondition 1 (X°C/ Z% RH)




TOBACCO PRODUCTFRESH



1Week 01

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*DWB=Dry weight basis. The DWB normalizes the results since starting moisture may vary.


Make sure LOQ is in the dataset - it is important.


A Shelf Life study dataset would shows analytes done in different test conditions with replicates over time points.  In the interest of brevity for this example, only moisture content using the TEST of Product Moisture (also known as Oven Volatile) percentage is shown in a sample of timepoints in two conditions with replicates.

Rows 1-9:Show the LBTEST of Product Moisture for Condition 1 (X°C/ Z% RH) which is shown in LBTSTCND. The sample of various timepoints that may be used in the testing for product moisture is reflected in LBTPT. The LBTPTNUM shows the numerical version of the planned timepoint. The REPNUM shows the incidence number of a test that is repeated within a given timeframe for the same test.
Rows 10-18:Show the LBTEST of Product Moisture for Condition 2 Condition 2 (A °C/ B %RH) across the same timepoints shown for Condition 1. The LBGRPID is used to tie together a block of related records in a single domain.

lb.xpt

lb.xpt

RowSTUDYIDDOMAINLBSEQLBGRPIDLBREFIDLBSPIDLBTESTCDLBTESTLBTSTCNDLBORRESLBORRESULBSTRESCLBSTRESNLBSTRESULBSPECLBSPCCNDLBMETHODLBANMETHLBTMTHSNLBSTNRCLBREPNUMLBTPTLBTPTNUM
1TOB07LB11


Product MoistureCondition 1 (X°C/ Z% RH)
%

%TOBACCO PRODUCTFRESH



1Week 01
2TOB07LB21


Product MoistureCondition 1 (X°C/ Z% RH)
%

%TOBACCO PRODUCTFRESH



2Week 01
3TOB07LB31


Product MoistureCondition 1 (X°C/ Z% RH)
%

%TOBACCO PRODUCTFRESH



3Week 01
4TOB07LB41


Product MoistureCondition 1 (X°C/ Z% RH)
%

%TOBACCO PRODUCTFRESH



1Week 84
5TOB07LB51


Product MoistureCondition 1 (X°C/ Z% RH)
%

%TOBACCO PRODUCTFRESH



2Week 84
6TOB07LB61


Product MoistureCondition 1 (X°C/ Z% RH)
%

%TOBACCO PRODUCTFRESH



3Week 84
7TOB07LB71


Product MoistureCondition 1 (X°C/ Z% RH)
%

%TOBACCO PRODUCTFRESH



1Week 489
8TOB07LB81


Product MoistureCondition 1 (X°C/ Z% RH)
%

%TOBACCO PRODUCTFRESH



2Week 489
9TOB07LB91


Product MoistureCondition 1 (X°C/ Z% RH)
%

%TOBACCO PRODUCTFRESH



3Week 489
10TOB07LB102


Product MoistureCondition 2 (A °C/ B %RH)
%

%TOBACCO PRODUCTFRESH



1Week 01
11TOB07LB112


Product MoistureCondition 2 (A °C/ B %RH)
%

%TOBACCO PRODUCTFRESH



2Week 01
12TOB07LB122


Product MoistureCondition 2 (A °C/ B %RH)
%

%TOBACCO PRODUCTFRESH



3Week 01
13TOB07LB132


Product MoistureCondition 2 (A °C/ B %RH)
%

%TOBACCO PRODUCTFRESH



1Week 84
14TOB07LB142


Product MoistureCondition 2 (A °C/ B %RH)
%

%TOBACCO PRODUCTFRESH



2Week 84
15TOB07LB152


Product MoistureCondition 2 (A °C/ B %RH)
%

%TOBACCO PRODUCTFRESH



3Week 84
16TOB07LB162


Product MoistureCondition 2 (A °C/ B %RH)
%

%TOBACCO PRODUCTFRESH



1Week 489
17TOB07LB172


Product MoistureCondition 2 (A °C/ B %RH)
%

%TOBACCO PRODUCTFRESH



2Week 489
18TOB07LB182


Product MoistureCondition 2 (A °C/ B %RH)
%

%TOBACCO PRODUCTFRESH



3Week 489
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