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Shelf life study has a protocol and provides the results of shelf life studies of tobacco Vapes products over time with different conditions and analytes. Generally there are many conditions with at least two with varying temperature, humidity, etc.
The initial table shows the a number of the analytes and test conditions used in Shelf Life studies for tobacco Vapes products for one testing condition at one timepoint and one replicate.
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| Row 1: | Shows the TTTEST of Product Moisture Potential Combustion Products which reflects the percentage of moisture potential for combustion in the E-Liquid substance for the condition noted in TTTSTCND which is Condition 1 (X°C/ Z% RH). Product Moisture is sometimes referred to as "Oven Volatiles". | | Rows 4, 6, 8 | Shows the NNK, NNN, and TSN tests with the tobacco product "as-is" using the TTSPCCND to show that the tobacco is "FRESH". | | E-Liquid Standard (Long Term) Condition. | | Rows 2, 3: | Shows the pH and Water Activity with the E-Liquid substance for the condition noted in TTTSTCND which is E-Liquid Standard (Long Term) Condition. | | Rows 4, 5, 6:Rows 5, 7, 9 | Shows the NNK, NNN, and TSN tests with the tobacco product as "Dry weight basis (DWB)" using the TTSPCCND to show that the tobacco is "DRIED".in the E-Liquid substance for the condition noted in TTTSTCND which is E-Liquid Standard (Long Term) Condition. | | Rows 7 - 9Rows 2-12: | Show the other analytes used in testing (pH, water activity, NNK, NNN, TSNA, etc.aerobic plate count, mold, and yeast) using the TTTEST and TTTESTCD variables. | |
| Dataset2 |
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| Row | STUDYID | DOMAIN | TTSEQ | TTREFID | SPTOBID | TTTESTCD | TTTEST | TTCAT | TTTSTCND | TTORRES | TTORRESU | TTSTRESC | TTSTRESN | TTSTRESU | TTSPEC | TTSPCCND | TTMETHOD | TTLLOQ | TTREPNUM | TTTPT | TTTPTNUM |
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| 1 | TOB07 | TT | 1 | VAP77777.1 | 111 | XXXXX | Potential Combustion Products | STABILITY STUDY | E-Liquid Standard (Long Term) Condition |
| % |
|
| % | E-LIQUID |
|
|
| 1 | Week 0 | 1 | | 2 | TOB07 | TT | 2 | VAP77777.1 |
| PH | pH | STABILITY STUDY | E-Liquid Standard (Long Term) Condition |
|
|
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|
| E-LIQUID |
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| 1 | Week 0 | 1 | | 3 | TOB07 | TT | 3 | VAP77777.1 |
| H2OACT | Water Activity | STABILITY STUDY | E-Liquid Standard (Long Term) Condition |
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| E-LIQUID |
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| 1 | Week 0 | 1 | | 4 | TOB07 | TT | 4 | VAP77777.1 |
| NNK | 4-(N-methyl-N-nitrosoamino)-1-(3-pyridyl)-1-butanone (NNK) | STABILITY STUDY | E-Liquid Standard (Long Term) Condition |
| ng/g |
|
| ng/g | E-LIQUID |
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|
| 1 | Week 0 | 1 | | 5 | TOB07 | TT | 6 | VAP77777.1 |
| NNN | N-nitrosonornicotine | STABILITY STUDY | E-Liquid Standard (Long Term) Condition |
| ng/g |
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| ng/g | E-LIQUID |
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|
| 1 | Week 0 | 1 | | 6 | TOB07 | TT | 8 | VAP77777.1 |
| TSNA | Tobacco-specific nitrosamines | STABILITY STUDY | E-Liquid Standard (Long Term) Condition |
| ng/g |
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| ng/g | E-LIQUID |
|
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| 1 | Week 0 | 1 | | 7 | TOB07 | TT | 10 | VAP77777.1 |
| AEBPLCT | Aerobic Plate Count | STABILITY STUDY | E-Liquid Standard (Long Term) Condition |
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| E-LIQUID |
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| 1 | Week 0 | 1 | | 8 | TOB07 | TT | 11 | VAP77777.1 |
| MOLD | Mold | STABILITY STUDY | E-Liquid Standard (Long Term) Condition |
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| E-LIQUID |
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| 1 | Week 0 | 1 | | 9 | TOB07 | TT | 12 | VAP77777.1 |
| YEAST | Yeast | STABILITY STUDY | E-Liquid Standard (Long Term) Condition |
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| E-LIQUID |
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| 1 | Week 0 | 1 |
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*DWB=Dry weight basis. The DWB normalizes the results since starting moisture may vary.
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| Rows 1-9: | Show the TTTEST of Potential Combusion Products for E-Liquid Standard (Long Term) Condition which is shown in TTTSTCND. The sample of various timepoints that may be used in the testing for Potential Combusion Products is reflected in TTTPT. The TTTPTNUM shows the numerical version of the planned timepoint. The REPNUM shows the incidence number of a test that is repeated within a given timeframe for the same test. | | Rows 10-18: | Show the TTTEST of Potential Combusion Products for E-Liquid Accelerated Aging Condition across the same timepoints. The TTGRPID is used to tie together a block of related records in a single domain. | | Rows 19-28: | Show the TTTEST of MIcrobiological for E-Vapor Standard Aerosol Condition across the same timepoints. The TTGRPID is used to tie together a block of related records in a single domain. | | Rows 29-36: | Show the TTTEST of MIcrobiological for E-Vapor Intense Aerosol Condition across the same timepoints. The TTGRPID is used to tie together a block of related records in a single domain. |
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| Dataset2 |
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| Row | | DOMAIN | TTSEQ | TTREFID | TTTESTCD | TTTEST | TTTSTCND | TTORRES | TTORRESU | TTSTRESC | TTSTRESN | TTSTRESU | TTSPEC | TTSPCCND | TTMETHOD | TTREPNUM | TTTPT | TTTPTNUM |
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| 1 | TOB07 | TT | 211 | VAP77777.1 | XXXXX | Potential Combustion Products | E-Liquid Standard (Long Term) Condition |
| % |
|
| % | E-LIQUID |
|
| 1 | Week 0 | 1 | | 2 | TOB07 | TT | 212 | VAP77777. |
2| 1 | XXXXX | Potential Combustion Products | E-Liquid Standard (Long Term) Condition |
| % |
|
| % | E-LIQUID |
|
| 2 | Week 0 | 1 | | 3 | TOB07 | TT | 213 | VAP77777. |
3| 1 | XXXXX | Potential Combustion Products | E-Liquid Standard (Long Term) Condition |
| % |
|
| % | E-LIQUID |
|
| 3 | Week 0 | 1 | | 4 | TOB07 | TT | 214 | VAP77777. |
4| 1 | XXXXX | Potential Combustion Products | E-Liquid Standard (Long Term) Condition |
| % |
|
| % | E-LIQUID |
|
| 1 | Week 8 | 4 | | 5 | TOB07 | TT | 215 | VAP77777. |
5| 1 | XXXXX | Potential Combustion Products | E-Liquid Standard (Long Term) Condition |
| % |
|
| % | E-LIQUID |
|
| 2 | Week 8 | 4 | | 6 | TOB07 | TT | 216 | VAP77777. |
6| 1 | XXXXX | Potential Combustion Products | E-Liquid Standard (Long Term) Condition |
| % |
|
| % | E-LIQUID |
|
| 3 | Week 8 | 4 | | 7 | TOB07 | TT | 217 | VAP77777. |
7| 1 | XXXXX | Potential Combustion Products | E-Liquid Standard (Long Term) Condition |
| % |
|
| % | E-LIQUID |
|
| 1 | Week 48 | 9 | | 8 | TOB07 | TT | 218 | VAP77777. |
8| 1 | XXXXX | Potential Combustion Products | E-Liquid Standard (Long Term) Condition |
| % |
|
| % | E-LIQUID |
|
| 2 | Week 48 | 9 | | 9 | TOB07 | TT | 219 | VAP77777. |
9| 1 | XXXXX | Potential Combustion Products | E-Liquid Standard (Long Term) Condition |
| % |
|
| % | E-LIQUID |
|
| 3 | Week 48 | 9 | | 10 | TOB07 | TT | 220 | VAP77777. |
10| 1 | YYYYYY | Potential Combustion Products | E-Liquid Accelerated Aging Condition |
| % |
|
| % | E-LIQUID |
|
| 1 | Week 0 | 1 | | 11 | TOB07 | TT | 221 | VAP77777. |
11| 1 | YYYYYY | Potential Combustion Products | E-Liquid Accelerated Aging Condition |
| % |
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| % | E-LIQUID |
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| 2 | Week 0 | 1 | | 12 | TOB07 | TT | 222 | VAP77777. |
12| 1 | YYYYYY | Potential Combustion Products | E-Liquid Accelerated Aging Condition |
| % |
|
| % | E-LIQUID |
|
| 3 | Week 0 | 1 | | 13 | TOB07 | TT | 223 | VAP77777. |
13| 1 | YYYYYY | Potential Combustion Products | E-Liquid Accelerated Aging Condition |
| % |
|
| % | E-LIQUID |
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| 1 | Week 8 | 4 | | 14 | TOB07 | TT | 224 | VAP77777. |
14| 1 | YYYYYY | Potential Combustion Products | E-Liquid Accelerated Aging Condition |
| % |
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| % | E-LIQUID |
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| 2 | Week 8 | 4 | | 15 | TOB07 | TT | 225 | VAP77777. |
15| 1 | YYYYYY | Potential Combustion Products | E-Liquid Accelerated Aging Condition |
| % |
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| % | E-LIQUID |
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| 3 | Week 8 | 4 | | 16 | TOB07 | TT | 226 | VAP77777. |
16| 1 | YYYYYY | Potential Combustion Products | E-Liquid Accelerated Aging Condition |
| % |
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| % | E-LIQUID |
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| 1 | Week 48 | 9 | | 17 | TOB07 | TT | 227 | VAP77777. |
17| 1 | YYYYYY | Potential Combustion Products | E-Liquid Accelerated Aging Condition |
| % |
|
| % | E-LIQUID |
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| 2 | Week 48 | 9 | | 18 | TOB07 | TT | 228 | VAP77777. |
18| 1 | YYYYYY | Potential Combustion Products | E-Liquid Accelerated Aging Condition |
| % |
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| % | E-LIQUID |
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| 3 | Week 48 | 9 | | 19 | TOB07 | TT | 229 | VAP77777.1 | AAAAA | Microbiological | E-Vapor Standard Aerosol Condition |
| % |
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| % | E-LIQUID |
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| 1 | Week 0 | 1 | | 20 | TOB07 | TT | 230 | VAP77777. |
2| 1 | AAAAA | Microbiological | E-Vapor Standard Aerosol Condition |
| % |
|
| % | E-LIQUID |
|
| 2 | Week 0 | 1 | | 21 | TOB07 | TT | 231 | VAP77777. |
3| 1 | AAAAA | Microbiological | E-Vapor Standard Aerosol Condition |
| % |
|
| % | E-LIQUID |
|
| 3 | Week 0 | 1 | | 22 | TOB07 | TT | 232 | VAP77777. |
4| 1 | AAAAA | Microbiological | E-Vapor Standard Aerosol Condition |
| % |
|
| % | E-LIQUID |
|
| 1 | Week 8 | 4 | | 23 | TOB07 | TT | 233 | VAP77777. |
5| 1 | AAAAA | Microbiological | E-Vapor Standard Aerosol Condition |
| % |
|
| % | E-LIQUID |
|
| 2 | Week 8 | 4 | | 24 | TOB07 | TT | 234 | VAP77777. |
6| 1 | AAAAA | Microbiological | E-Vapor Standard Aerosol Condition |
| % |
|
| % | E-LIQUID |
|
| 3 | Week 8 | 4 | | 25 | TOB07 | TT | 235 | VAP77777. |
7| 1 | AAAAA | Microbiological | E-Vapor Standard Aerosol Condition |
| % |
|
| % | E-LIQUID |
|
| 1 | Week 48 | 9 | | 26 | TOB07 | TT | 236 | VAP77777. |
8| 1 | AAAAA | Microbiological | E-Vapor Standard Aerosol Condition |
| % |
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| % | E-LIQUID |
|
| 2 | Week 48 | 9 | | 27 | TOB07 | TT | 237 | VAP77777. |
9| 1 | AAAAA | Microbiological | E-Vapor Standard Aerosol Condition |
| % |
|
| % | E-LIQUID |
|
| 3 | Week 48 | 9 | | 28 | TOB07 | TT | 238 | VAP77777. |
10| 1 | BBBBBB | Microbiological | E-Vapor Standard Aerosol Condition |
| % |
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| % | E-LIQUID |
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| 1 | Week 0 | 1 | | 29 | TOB07 | TT | 239 | VAP77777. |
11| 1 | BBBBBB | Microbiological | E-Vapor Intense Aerosol Condition |
| % |
|
| % | E-LIQUID |
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| 2 | Week 0 | 1 | | 30 | TOB07 | TT | 240 | VAP77777. |
12| 1 | BBBBBB | Microbiological | E-Vapor Intense Aerosol Condition |
| % |
|
| % | E-LIQUID |
|
| 3 | Week 0 | 1 | | 31 | TOB07 | TT | 241 | VAP77777. |
13| 1 | BBBBBB | Microbiological | E-Vapor Intense Aerosol Condition |
| % |
|
| % | E-LIQUID |
|
| 1 | Week 8 | 4 | | 32 | TOB07 | TT | 242 | VAP77777. |
14| 1 | BBBBBB | Microbiological | E-Vapor Intense Aerosol Condition |
| % |
|
| % | E-LIQUID |
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| 2 | Week 8 | 4 | | 33 | TOB07 | TT | 243 | VAP77777. |
15| 1 | BBBBBB | Microbiological | E-Vapor Intense Aerosol Condition |
| % |
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| % | E-LIQUID |
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| 3 | Week 8 | 4 | | 34 | TOB07 | TT | 244 | VAP77777. |
16| 1 | BBBBBB | Microbiological | E-Vapor Intense Aerosol Condition |
| % |
|
| % | E-LIQUID |
|
| 1 | Week 48 | 9 | | 35 | TOB07 | TT | 245 | VAP77777. |
17| 1 | BBBBBB | Microbiological | E-Vapor Intense Aerosol Condition |
| % |
|
| % | E-LIQUID |
|
| 2 | Week 48 | 9 | | 36 | TOB07 | TT | 246 | VAP77777. |
18| 1 | BBBBBB | Microbiological | E-Vapor Intense Aerosol Condition |
| % |
|
| % | E-LIQUID |
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| 3 | Week 48 | 9 |
|
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