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The initial table shows the a number of the analytes and test conditions used in Shelf Life studies for tobacco products for one testing condition at one timepoint and one replicate.
For Specimen - could use Plant based material; Synthetic material (codelist has swabbed material); For Specimen Condition- could use DRIED, FRESH, CONCENTRATED,
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Row 1: | Shows the LBTEST of Product Moisture which reflects the percentage of moisture in the substance for the condition noted in LBTSTCND which is Condition 1 (X°C/ Z% RH). Product Moisture is sometimes referred to as "Oven Volatiles". | Rows 2-12: | Show the analytes used in testing. | |
Dataset2 |
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Row | STUDYID | DOMAIN | LBSEQ | LBREFID | LBSPID | LBTESTCD | LBTEST | LBTSTCND | LBORRES | LBORRESU | LBSTRESC | LBSTRESN | LBSTRESU | LBSPEC | LBSPCCND | LBMETHOD | LBANMETH | LBTMTHSN | LBSTNRC | LBREPNUM | LBTPT | LBTPTNUM |
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1 | TOB07 | LB | 1 |
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| Product Moisture | Condition 1 (X°C/ Z% RH) |
| % |
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| % | MATERIAL | FRESH |
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| 1 | Week 1 | 1 | 2 | TOB07 | LB | 2 |
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| pH | Condition 1 (X°C/ Z% RH) |
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| MATERIAL | FRESH |
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| 1 | Week 1 | 1 | 3 | TOB07 | LB | 3 |
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| Water Activity | Condition 1 (X°C/ Z% RH) |
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| MATERIAL | FRESH |
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| 1 | Week 1 | 1 | 4 | TOB07 | LB | 4 |
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| NNK-as is | Condition 1 (X°C/ Z% RH) |
| ng/g |
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| ng/g | MATERIAL | FRESH |
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| 1 | Week 1 | 1 | 5 | TOB07 | LB | 5 |
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| NNK-DWB* | Condition 1 (X°C/ Z% RH) |
| ng/g |
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| ng/g | MATERIAL | DRIED |
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| 1 | Week 1 | 1 | 6 | TOB07 | LB | 6 |
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| NNN-as is | Condition 1 (X°C/ Z% RH) |
| ng/g |
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| ng/g | MATERIAL | FRESH |
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| 1 | Week 1 | 1 | 7 | TOB07 | LB | 7 |
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| NNK-DWB | Condition 1 (X°C/ Z% RH) |
| ng/g |
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| ng/g | MATERIAL | DRIED |
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| 1 | Week 1 | 1 | 8 | TOB07 | LB | 8 |
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| TSNA -as is | Condition 1 (X°C/ Z% RH) |
| ng/g |
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| ng/g | MATERIAL | DRIED |
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| 1 | Week 1 | 1 | 9 | TOB07 | LB | 9 |
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| TSNA -DWB | Condition 1 (X°C/ Z% RH) |
| ng/g |
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| ng/g | MATERIAL | DRIED |
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| 1 | Week 1 | 1 | 10 | TOB07 | LB | 10 |
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| Aerobic Plate Count | Condition 1 (X°C/ Z% RH) |
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| MATERIAL | FRESH |
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| 1 | Week 1 | 1 | 11 | TOB07 | LB | 11 |
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| Mold | Condition 1 (X°C/ Z% RH) |
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| MATERIAL | FRESH |
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| 1 | Week 1 | 1 | 12 | TOB07 | LB | 12 |
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| Yeast | Condition 1 (X°C/ Z% RH) |
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| MATERIAL | FRESH |
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| 1 | Week 1 | 1 |
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*DWB=Dry weight basis. The DWB normalizes the results since starting moisture may vary.
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Rows 1-9: | Show the LBTEST of Product Moisture for Condition 1 (X°C/ Z% RH) which is shown in LBTSTCND. The sample of various timepoints that may be used in the testing for product moisture is reflected in LBTPT. The LBTPTNUM shows the numerical version of the planned timepoint. The REPNUM shows the incidence number of a test that is repeated within a given timeframe for the same test. | Rows 10-18: | Show the LBTEST of Product Moisture for Condition 2 Condition 2 (A °C/ B %RH) across the same timepoints shown for Condition 1. The LBGRPID is used to tie together a block of related records in a single domain. | |
Dataset2 |
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Row | STUDYID | DOMAIN | LBSEQ | LBGRPID | LBREFID | LBSPID | LBTESTCD | LBTEST | LBTSTCND | LBORRES | LBORRESU | LBSTRESC | LBSTRESN | LBSTRESU | LBSPEC | LBSPCCND | LBMETHOD | LBANMETH | LBTMTHSN | LBSTNRC | LBREPNUM | LBTPT | LBTPTNUM |
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1 | TOB07 | LB | 1 | 1 |
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| Product Moisture | Condition 1 (X°C/ Z% RH) |
| % |
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| % | MATERIAL | FRESH |
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| 1 | Week 0 | 1 | 2 | TOB07 | LB | 2 | 1 |
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| Product Moisture | Condition 1 (X°C/ Z% RH) |
| % |
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| % | MATERIAL | FRESH |
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| 2 | Week 0 | 1 | 3 | TOB07 | LB | 3 | 1 |
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| Product Moisture | Condition 1 (X°C/ Z% RH) |
| % |
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| % | MATERIAL | FRESH |
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| 3 | Week 0 | 1 | 4 | TOB07 | LB | 4 | 1 |
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| Product Moisture | Condition 1 (X°C/ Z% RH) |
| % |
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| % | MATERIAL | FRESH |
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| 1 | Week 8 | 4 | 5 | TOB07 | LB | 5 | 1 |
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| Product Moisture | Condition 1 (X°C/ Z% RH) |
| % |
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| % | MATERIAL | FRESH |
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| 2 | Week 8 | 4 | 6 | TOB07 | LB | 6 | 1 |
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| Product Moisture | Condition 1 (X°C/ Z% RH) |
| % |
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| % | MATERIAL | FRESH |
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| 3 | Week 8 | 4 | 7 | TOB07 | LB | 7 | 1 |
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| Product Moisture | Condition 1 (X°C/ Z% RH) |
| % |
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| % | MATERIAL | FRESH |
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| 1 | Week 48 | 9 | 8 | TOB07 | LB | 8 | 1 |
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| Product Moisture | Condition 1 (X°C/ Z% RH) |
| % |
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| % | MATERIAL | FRESH |
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| 2 | Week 48 | 9 | 9 | TOB07 | LB | 9 | 1 |
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| Product Moisture | Condition 1 (X°C/ Z% RH) |
| % |
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| % | MATERIAL | FRESH |
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| 3 | Week 48 | 9 | 10 | TOB07 | LB | 10 | 2 |
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| Product Moisture | Condition 2 (A °C/ B %RH) |
| % |
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| % | MATERIAL | FRESH |
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| 1 | Week 0 | 1 | 11 | TOB07 | LB | 11 | 2 |
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| Product Moisture | Condition 2 (A °C/ B %RH) |
| % |
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| % | MATERIAL | FRESH |
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| 2 | Week 0 | 1 | 12 | TOB07 | LB | 12 | 2 |
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| Product Moisture | Condition 2 (A °C/ B %RH) |
| % |
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| % | MATERIAL | FRESH |
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| 3 | Week 0 | 1 | 13 | TOB07 | LB | 13 | 2 |
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| Product Moisture | Condition 2 (A °C/ B %RH) |
| % |
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| % | MATERIAL | FRESH |
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| 1 | Week 8 | 4 | 14 | TOB07 | LB | 14 | 2 |
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| Product Moisture | Condition 2 (A °C/ B %RH) |
| % |
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| % | MATERIAL | FRESH |
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| 2 | Week 8 | 4 | 15 | TOB07 | LB | 15 | 2 |
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| Product Moisture | Condition 2 (A °C/ B %RH) |
| % |
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| % | MATERIAL | FRESH |
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| 3 | Week 8 | 4 | 16 | TOB07 | LB | 16 | 2 |
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| Product Moisture | Condition 2 (A °C/ B %RH) |
| % |
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| % | MATERIAL | FRESH |
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| 1 | Week 48 | 9 | 17 | TOB07 | LB | 17 | 2 |
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| Product Moisture | Condition 2 (A °C/ B %RH) |
| % |
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| % | MATERIAL | FRESH |
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| 2 | Week 48 | 9 | 18 | TOB07 | LB | 18 | 2 |
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| Product Moisture | Condition 2 (A °C/ B %RH) |
| % |
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| % | MATERIAL | FRESH |
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| 3 | Week 48 | 9 |
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